Information card for entry 4070127

Structure parameters

• Formula: C47.92 H71.73 Bi Ge N4 O Si2
• Calculated formula: C47.922 H71.727 Bi Ge N4 O Si2
• Title of publication: Synthesis and Structural Characterization of Heterobimetallic Bismuth Complexes with Main Group and Transition Metals
• Authors of publication: Nekoueishahraki, Bijan; Jana, Anukul; Roesky, Herbert W.; Mishra, Lallan; Stern, Daniel; Stalke, Dietmar
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 19
• Pages of publication: 5733
• a: 22.6065 ± 0.0005 Å
• b: 21.8965 ± 0.0005 Å
• c: 22.8045 ± 0.0004 Å
• α: 90°
• β: 117.56 ± 0.001°
• γ: 90°
• Cell volume: 10007.4 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0223
• Residual factor for significantly intense reflections: 0.0192
• Weighted residual factors for significantly intense reflections: 0.0438
• Weighted residual factors for all reflections included in the refinement: 0.045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No