Information card for entry 4073967

Structure parameters

• Formula: C24 H38 N4 W
• Calculated formula: C24 H38 N4 W
• Title of publication: Bis(imido) W(VI) Complexes Chelated by N,N′-Disubstituted 1,8-Diamidonaphthalene: An Analysis of Bonding, Isocyanate Insertion, and Al-Me Transfer
• Authors of publication: Lavoie, Nathalie; Ong, Tiow-Gan; Gorelsky, Serge I.; Korobkov, Ilia; Yap, Glenn P. A.; Richeson, Darrin S.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 26
• Pages of publication: 6586
• a: 9.86 ± 0.004 Å
• b: 14.171 ± 0.005 Å
• c: 18.738 ± 0.007 Å
• α: 98.619 ± 0.006°
• β: 102.019 ± 0.006°
• γ: 93.095 ± 0.006°
• Cell volume: 2522 ± 1.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0893
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No