Crystallography Open Database

Information card for entry 4074209

Preview

Coordinates	4074209.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H33 As Os
Calculated formula	C28 H33 As Os
Title of publication	Synthesis and Characterization of Osmium(IV) Polyhydride Complexes of Stoichiometry (C5Me5)OsH3(L). Crystal Structures of (C5Me5)OsH3(AsPh3) and (C5Me5)OsH3(PPh3)
Authors of publication	Gross, Christopher L.; Girolami, Gregory S.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	20
Pages of publication	4792
a	8.5812 ± 0.0003 Å
b	9.2527 ± 0.0003 Å
c	17.3789 ± 0.0006 Å
α	93.04°
β	101.095 ± 0.001°
γ	113.856 ± 0.001°
Cell volume	1225.16 ± 0.07 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0352
Residual factor for significantly intense reflections	0.0268
Weighted residual factors for significantly intense reflections	0.0575
Weighted residual factors for all reflections included in the refinement	0.0615
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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