Information card for entry 4074290

Structure parameters

• Common name: Compound 5
• Formula: C72 H56 B Cl6 F24 Mo N3
• Calculated formula: C72 H56 B Cl6 F24 Mo N3
• Title of publication: Cationic Imido Alkylidene Complexes of Molybdenum Supported by β-Diketonate and β-Diketiminate Ligands
• Authors of publication: Tonzetich, Zachary J.; Jiang, Annie J.; Schrock, Richard R.; Müller, Peter
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 20
• Pages of publication: 4725
• a: 12.701 ± 0.001 Å
• b: 15.1067 ± 0.0012 Å
• c: 19.2234 ± 0.0013 Å
• α: 93.61 ± 0.002°
• β: 96.934 ± 0.002°
• γ: 92.006 ± 0.002°
• Cell volume: 3650.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1238
• Weighted residual factors for all reflections included in the refinement: 0.1393
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No