Information card for entry 4074291

Structure parameters

• Formula: C24 H72 Ca Mg N4 Si8
• Calculated formula: C24.054 H72.162 Ca Mg N4 Si8
• Title of publication: Heterodimetallic Alkaline Earth Metal Amides: Synthesis, Structure, and Solvent-Induced Charge Separation of Homoleptic Calcium−Magnesium Hexamethyldisilazide
• Authors of publication: Wendell, Lauren T.; Bender, John; He, Xuyang; Noll, Bruce C.; Henderson, Kenneth W.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 21
• Pages of publication: 4953
• a: 9.164 ± 0.0003 Å
• b: 12.108 ± 0.0004 Å
• c: 21.654 ± 0.0008 Å
• α: 87.541 ± 0.002°
• β: 85.78 ± 0.003°
• γ: 69.55 ± 0.002°
• Cell volume: 2244.77 ± 0.14 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1102
• Weighted residual factors for all reflections included in the refinement: 0.1243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No