Information card for entry 4074913

Structure parameters

• Formula: C78 H136 Cl4 N8 Nd4 O4 Si8
• Calculated formula: C78 H104 Cl4 N8 Nd4 O4 Si8
• Title of publication: Metallomacrocycle Complexes of Lanthanides with Bridged Amide Ligands: Syntheses and Molecular Structures of [{μ2-p-(Me3SiN)2C6H4}YbCl(THF)2]2and [{μ2-p-(Me3SiN)2C6H4}Nd(μ2-Cl)(THF)]42PhMe
• Authors of publication: Zhao, Bei; Li, Honghai; Shen, Qi; Zhang, Yong; Yao, Yingming; Lu, Chengrong
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 7
• Pages of publication: 1824
• a: 13.8273 ± 0.0015 Å
• b: 14.2373 ± 0.0011 Å
• c: 14.796 ± 0.001 Å
• α: 61.759 ± 0.005°
• β: 85.629 ± 0.009°
• γ: 86.579 ± 0.009°
• Cell volume: 2557.7 ± 0.4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.0995
• Weighted residual factors for all reflections included in the refinement: 0.1079
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No