Information card for entry 4074914

Structure parameters

• Formula: C40 H76 Cl2 N4 O4 Si4 Yb2
• Calculated formula: C40 H76 Cl2 N4 O4 Si4 Yb2
• SMILES: c12ccc(cc1)N([Si](C)(C)C)[Yb](N(c1ccc(cc1)N([Yb](N2[Si](C)(C)C)([O]1CCCC1)([O]1CCCC1)Cl)[Si](C)(C)C)[Si](C)(C)C)([O]1CCCC1)([O]1CCCC1)Cl
• Title of publication: Metallomacrocycle Complexes of Lanthanides with Bridged Amide Ligands: Syntheses and Molecular Structures of [{μ2-p-(Me3SiN)2C6H4}YbCl(THF)2]2and [{μ2-p-(Me3SiN)2C6H4}Nd(μ2-Cl)(THF)]42PhMe
• Authors of publication: Zhao, Bei; Li, Honghai; Shen, Qi; Zhang, Yong; Yao, Yingming; Lu, Chengrong
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 7
• Pages of publication: 1824
• a: 25.127 ± 0.003 Å
• b: 12.0839 ± 0.0013 Å
• c: 17.4643 ± 0.0019 Å
• α: 90°
• β: 93.481 ± 0.003°
• γ: 90°
• Cell volume: 5292.9 ± 1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0561
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.135
• Goodness-of-fit parameter for all reflections included in the refinement: 1.232
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No