Information card for entry 4075533

Structure parameters

• Formula: C13 H30 Cl P Pd
• Calculated formula: C13 H30 Cl P Pd
• SMILES: [Pd](Cl)(C)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C
• Title of publication: Syntheses and Structures of Bulky Monophosphine-Ligated Methylpalladium Complexes: Application to Homo- and Copolymerization of Norbornene and/or Methoxycarbonylnorbornene
• Authors of publication: Yamashita, Makoto; Takamiya, Ikuko; Jin, Koichiro; Nozaki, Kyoko
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 19
• Pages of publication: 4588
• a: 8.551 ± 0.009 Å
• b: 9.521 ± 0.009 Å
• c: 9.873 ± 0.011 Å
• α: 91.59 ± 0.02°
• β: 91.034 ± 0.02°
• γ: 94.29 ± 0.02°
• Cell volume: 801.1 ± 1.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.0918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.213
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No