Crystallography Open Database

Information card for entry 4075534

Preview

Coordinates	4075534.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H25 Cl4 P Pd
Calculated formula	C23 H25 Cl4 P Pd
Title of publication	Syntheses and Structures of Bulky Monophosphine-Ligated Methylpalladium Complexes: Application to Homo- and Copolymerization of Norbornene and/or Methoxycarbonylnorbornene
Authors of publication	Yamashita, Makoto; Takamiya, Ikuko; Jin, Koichiro; Nozaki, Kyoko
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	19
Pages of publication	4588
a	9.385 ± 0.018 Å
b	10.88 ± 0.02 Å
c	11.97 ± 0.02 Å
α	81.62 ± 0.09°
β	80.91 ± 0.09°
γ	83.78 ± 0.09°
Cell volume	1189 ± 4 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0398
Residual factor for significantly intense reflections	0.0357
Weighted residual factors for significantly intense reflections	0.0809
Weighted residual factors for all reflections included in the refinement	0.0823
Goodness-of-fit parameter for all reflections included in the refinement	0.961
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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