Information card for entry 4076270

Structure parameters

• Common name: mnh18
• Formula: C20 H33 K Mn O8
• Calculated formula: C20 H32 K Mn O8
• Title of publication: Structure of the Elusive Hydrido(methylcyclopentadienyl)dicarbonylmanganate(I) Anion, [(η5-C5H4Me)Mn(CO)2H]-, as Determined by Single-Crystal X-ray Diffraction
• Authors of publication: Chatterton, Nicholas P.; Guilera, Gemma; McGrady, G. Sean
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Journal issue: 5
• Pages of publication: 1165
• a: 9.467 ± 0.0019 Å
• b: 13.707 ± 0.003 Å
• c: 17.709 ± 0.005 Å
• α: 89.36 ± 0.011°
• β: 88.989 ± 0.011°
• γ: 89.096 ± 0.015°
• Cell volume: 2297.2 ± 0.9 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0801
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0683
• Weighted residual factors for all reflections included in the refinement: 0.078
• Goodness-of-fit parameter for all reflections included in the refinement: 0.977
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No