Information card for entry 4076271

Structure parameters

• Formula: C37 H38 Cl2 N3 Rh2
• Calculated formula: C37 H38 Cl2 N3 Rh2
• Title of publication: Bis(imino)carbazolide Complexes of Rhodium: Highly Nucleophilic Ligands Exerting a Dramatic Accelerating Effect on MeI Oxidative Addition
• Authors of publication: Gaunt, Joseph A.; Gibson, Vernon C.; Haynes, Anthony; Spitzmesser, Stefan K.; White, Andrew J. P.; Williams, David J.
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Journal issue: 5
• Pages of publication: 1015
• a: 11.3599 ± 0.0004 Å
• b: 18.0866 ± 0.0011 Å
• c: 18.219 ± 0.002 Å
• α: 75.749 ± 0.006°
• β: 74.98 ± 0.008°
• γ: 78.884 ± 0.005°
• Cell volume: 3470.7 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0807
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for all reflections: 0.1445
• Weighted residual factors for significantly intense reflections: 0.1259
• Goodness-of-fit parameter for all reflections: 1.035
• Goodness-of-fit parameter for significantly intense reflections: 1.087
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No