Information card for entry 4077252

Structure parameters

• Formula: C88 H100 B P4 Rh Si4
• Calculated formula: C88 H100 B P4 Rh Si4
• Title of publication: Increasing the Lipophilic Character of Tetraphenylborate Anions through Silyl Substituents
• Authors of publication: van den Broeke, Joep; Lutz, Martin; Kooijman, Huub; Spek, Anthony L.; Deelman, Berth-Jan; van Koten, Gerard
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 10
• Pages of publication: 2114
• a: 14.7259 ± 0.0002 Å
• b: 20.1809 ± 0.0002 Å
• c: 16.4196 ± 0.0002 Å
• α: 90°
• β: 96.5775 ± 0.0004°
• γ: 90°
• Cell volume: 4847.49 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0407
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No