Information card for entry 4077268

Structure parameters

• Formula: C36 H76 Li N4 Si3 Ta
• Calculated formula: C36 H76 Li N4 Si3 Ta
• Title of publication: Alkyl and Alkylidene Tantalum−Lithium Complexes Supported by an Anionic Triazacyclononane Ligand
• Authors of publication: Schmidt, Joseph A. R.; Chmura, Stephen A.; Arnold, John
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 6
• Pages of publication: 1062
• a: 17.476 ± 0.003 Å
• b: 11.198 ± 0.002 Å
• c: 21.84 ± 0.004 Å
• α: 90°
• β: 99.506 ± 0.004°
• γ: 90°
• Cell volume: 4215.3 ± 1.3 ų
• Cell temperature: 154.2 K
• Ambient diffraction temperature: 154.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.033
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0322
• Goodness-of-fit parameter for significantly intense reflections: 0.797
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No