Information card for entry 4077269

Structure parameters

• Formula: C32 H64 Li N4 Si2 Ta
• Calculated formula: C32 H64 Li N4 Si2 Ta
• Title of publication: Alkyl and Alkylidene Tantalum−Lithium Complexes Supported by an Anionic Triazacyclononane Ligand
• Authors of publication: Schmidt, Joseph A. R.; Chmura, Stephen A.; Arnold, John
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 6
• Pages of publication: 1062
• a: 10.572 ± 0.001 Å
• b: 18.131 ± 0.002 Å
• c: 20.524 ± 0.002 Å
• α: 90°
• β: 103.789 ± 0.002°
• γ: 90°
• Cell volume: 3820.7 ± 0.7 ų
• Cell temperature: 154.2 K
• Ambient diffraction temperature: 154.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.169
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.0894
• Goodness-of-fit parameter for significantly intense reflections: 1.78
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No