Crystallography Open Database

Information card for entry 4077751

Preview

Coordinates	4077751.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H77 Cl2 Gd4 N5 O3 Si4
Calculated formula	C56 H64 Cl2 Gd4 N5 O3 Si4
Title of publication	Synthesis and Structure of the First Tetranuclear Organolanthanide Cluster Containing aμ4-Imido Group
Authors of publication	Xie, Zuowei; Wang, Shaowu; Yang, Qingchuan; Mak, Thomas C. W.
Journal of publication	Organometallics
Year of publication	1999
Journal volume	18
Journal issue	9
Pages of publication	1578
a	21.625 ± 0.0015 Å
b	19.226 ± 0.0015 Å
c	15.125 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	6288.4 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	41
Hermann-Mauguin space group symbol	A b a 2
Hall space group symbol	A 2 -2ab
Residual factor for all reflections	0.0642
Residual factor for significantly intense reflections	0.0631
Weighted residual factors for all reflections	0.1597
Weighted residual factors for significantly intense reflections	0.1583
Goodness-of-fit parameter for all reflections	1.058
Goodness-of-fit parameter for significantly intense reflections	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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