Information card for entry 4079757

Structure parameters

• Formula: C36 H25 Ge N O10 Os3
• Calculated formula: C36 H25 Ge N O10 Os3
• SMILES: [Os]12([Os]([Os]1(C#[O])(C#[O])(C#[O])C#[O])([H]2)([N]#CC)(C#[O])(C#[O])C#[O])([Ge](c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O].c1ccccc1
• Title of publication: Osmium‒Germanium and Osmium‒Germanium‒Gold Carbonyl Cluster Complexes: Syntheses, Structures, Bonding, and Reactivity
• Authors of publication: Adams, Richard D.; Kan, Yuwei; Zhang, Qiang
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 24
• Pages of publication: 8639
• a: 11.1548 ± 0.0004 Å
• b: 13.7581 ± 0.0005 Å
• c: 14.1494 ± 0.0005 Å
• α: 65.73 ± 0.001°
• β: 71.569 ± 0.001°
• γ: 85.375 ± 0.001°
• Cell volume: 1874.97 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.0515
• Weighted residual factors for all reflections included in the refinement: 0.0558
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No