Information card for entry 4079758

Structure parameters

• Formula: C46 H32 Ge2 O10 Os3
• Calculated formula: C46 H32 Ge2 O10 Os3
• SMILES: [Os]123([Os]([Os]1([H]2)(C#[O])(C#[O])(C#[O])C#[O])([Ge](c1ccccc1)(c1ccccc1)c1ccccc1)([H]3)(C#[O])(C#[O])C#[O])([Ge](c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O]
• Title of publication: Osmium‒Germanium and Osmium‒Germanium‒Gold Carbonyl Cluster Complexes: Syntheses, Structures, Bonding, and Reactivity
• Authors of publication: Adams, Richard D.; Kan, Yuwei; Zhang, Qiang
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 24
• Pages of publication: 8639
• a: 18.223 ± 0.0011 Å
• b: 17.1315 ± 0.0011 Å
• c: 28.6054 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8930.2 ± 1 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0594
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0503
• Weighted residual factors for all reflections included in the refinement: 0.0557
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No