Information card for entry 4079759

Structure parameters

• Formula: C29 H10 Ge O17 Os5
• Calculated formula: C29 H10 Ge O17 Os5
• SMILES: [Os]123([Os]4([Os]2([Os]1(C#[O])(C#[O])(C#[O])C#[O])([Os]4(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])([Ge]3(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Osmium‒Germanium and Osmium‒Germanium‒Gold Carbonyl Cluster Complexes: Syntheses, Structures, Bonding, and Reactivity
• Authors of publication: Adams, Richard D.; Kan, Yuwei; Zhang, Qiang
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 24
• Pages of publication: 8639
• a: 10.0493 ± 0.0003 Å
• b: 10.1132 ± 0.0003 Å
• c: 18.3249 ± 0.0005 Å
• α: 83.704 ± 0.001°
• β: 86.876 ± 0.001°
• γ: 73.42 ± 0.001°
• Cell volume: 1773.65 ± 0.09 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1003
• Weighted residual factors for all reflections included in the refinement: 0.112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No