Information card for entry 4079894

Structure parameters

• Common name: MePhSi(ON[Me]O)
• Chemical name: 2,4,8,10-Tetra-tert-butyl-6,12-dimethyl-6-phenyl-12H- dibenzo[d,g][1,3,6,2]dioxazasilocine
• Formula: C36 H51 N O2 Si
• Calculated formula: C36 H51 N O2 Si
• Title of publication: Migrations of Alkyl and Aryl Groups from Silicon to Nitrogen in Silylated Aryloxyiminoquinones
• Authors of publication: Shekar, Sukesh; Brown, Seth N.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 2
• Pages of publication: 556
• a: 10.8488 ± 0.0014 Å
• b: 10.8977 ± 0.0015 Å
• c: 15.012 ± 0.002 Å
• α: 78.879 ± 0.002°
• β: 73.065 ± 0.002°
• γ: 75.628 ± 0.002°
• Cell volume: 1630.7 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0957
• Weighted residual factors for all reflections included in the refinement: 0.1017
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No