Information card for entry 4084011

Structure parameters

• Formula: C23 H10 Br O11 Os3 Sb
• Calculated formula: C23 H10 Br O11 Os3 Sb
• SMILES: [Os]1([Os]([Os]([Sb]1(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(Br)(C#[O])(C#[O])C#[O]
• Title of publication: Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings
• Authors of publication: Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3867
• a: 10.0329 ± 0.0003 Å
• b: 16.4034 ± 0.0003 Å
• c: 16.9501 ± 0.0003 Å
• α: 90°
• β: 98.453 ± 0.002°
• γ: 90°
• Cell volume: 2759.24 ± 0.11 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.069
• Goodness-of-fit parameter for all reflections included in the refinement: 0.925
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No