Information card for entry 4084012

Structure parameters

• Formula: C22 H10 Cl O10 Os3 Sb
• Calculated formula: C22 H10 Cl O10 Os3 Sb
• SMILES: [Os]12([Os]([Os]([Sb]1(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])[Cl]2)(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings
• Authors of publication: Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3867
• a: 9.1927 ± 0.0008 Å
• b: 12.0103 ± 0.0008 Å
• c: 12.4195 ± 0.0009 Å
• α: 82.944 ± 0.003°
• β: 84.716 ± 0.002°
• γ: 84.485 ± 0.002°
• Cell volume: 1350.04 ± 0.18 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0275
• Residual factor for significantly intense reflections: 0.0235
• Weighted residual factors for significantly intense reflections: 0.0646
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.294
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No