Information card for entry 4085430

Structure parameters

• Formula: C99 H139 K3 N6 Si3
• Calculated formula: C99 H139 K3 N6 Si3
• Title of publication: Group 1 Complexes of an (Amido-amino)silane and Their Use in the Synthesis of the Bi(III) Amide, Bi(Me2Si{NAr}{N(H)Ar})Cl2(Ar = 2,6-i-Pr2C6H3)
• Authors of publication: Schwamm, Ryan J.; Coles, Martyn P.; Fitchett, Christopher M.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2500
• a: 16.6239 ± 0.0003 Å
• b: 17.1021 ± 0.0004 Å
• c: 17.7075 ± 0.0004 Å
• α: 84.9008 ± 0.0019°
• β: 83.8507 ± 0.0018°
• γ: 76.4098 ± 0.0019°
• Cell volume: 4854.61 ± 0.19 ų
• Cell temperature: 120.01 ± 0.1 K
• Ambient diffraction temperature: 120.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0761
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1844
• Weighted residual factors for all reflections included in the refinement: 0.195
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No