Information card for entry 4086445

Structure parameters

• Formula: C76 H88 F4 Ga4 O8 Si8
• Calculated formula: C76 H88 F4 Ga4 O8 Si8
• Title of publication: Gallium‒Gallium Bonds as Key Building Blocks for the Formation of Large Organometallic Macrocycles, on the Way to a Mesoporous Molecule
• Authors of publication: Uhl, Werner; Fick, Anna-Christina; Spies, Thomas; Geiseler, Gertraud; Harms, Klaus
• Journal of publication: Organometallics
• Year of publication: 2004
• Journal volume: 23
• Journal issue: 1
• Pages of publication: 72 - 75
• a: 14.124 ± 0.001 Å
• b: 17.805 ± 0.001 Å
• c: 20.02 ± 0.002 Å
• α: 90.266 ± 0.006°
• β: 105.679 ± 0.006°
• γ: 107.488 ± 0.006°
• Cell volume: 4603 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1056
• Residual factor for significantly intense reflections: 0.0725
• Weighted residual factors for significantly intense reflections: 0.2082
• Weighted residual factors for all reflections included in the refinement: 0.2198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.296
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No