Information card for entry 4086497

Structure parameters

• Formula: C25 H62 N2 Si6 Yb
• Calculated formula: C25 H62 N2 Si6 Yb
• SMILES: [Yb]1(C([SiH](C)C)([Si](C)(C)[H]1)[SiH](C)C)(C([SiH](C)C)([SiH](C)C)[SiH](C)C)=C1N(C(C)(C)C)C=CN1C(C)(C)C
• Title of publication: Homoleptic Divalent Dialkyl Lanthanide-Catalyzed Cross-Dehydrocoupling of Silanes and Amines
• Authors of publication: Pindwal, Aradhana; Ellern, Arkady; Sadow, Aaron D.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 1674
• a: 19.9684 ± 0.0016 Å
• b: 16.7745 ± 0.0014 Å
• c: 22.8246 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7645.3 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0601
• Weighted residual factors for all reflections included in the refinement: 0.0679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No