Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P–E···Te(II,IV) Bonding Situations (E = O, S, Se)
Authors of publication
Hupf, Emanuel; Do, Truong Giang; Nordheider, Andreas; Wehrhahn, Maren; Sanz Camacho, Paula; Ashbrook, Sharon E.; Lork, Enno; Slawin, Alexandra M. Z.; Mebs, Stefan; Woollins, J. Derek; Beckmann, Jens
Journal of publication
Organometallics
Year of publication
2017
a
13.7011 ± 0.0004 Å
b
14.8695 ± 0.0004 Å
c
15.7854 ± 0.0005 Å
α
99.809 ± 0.002°
β
110.93 ± 0.002°
γ
106.55 ± 0.002°
Cell volume
2743.09 ± 0.16 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0932
Residual factor for significantly intense reflections
0.0587
Weighted residual factors for significantly intense reflections
0.1389
Weighted residual factors for all reflections included in the refinement
0.152
Goodness-of-fit parameter for all reflections included in the refinement
