Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P–E···Te(II,IV) Bonding Situations (E = O, S, Se)
Authors of publication
Hupf, Emanuel; Do, Truong Giang; Nordheider, Andreas; Wehrhahn, Maren; Sanz Camacho, Paula; Ashbrook, Sharon E.; Lork, Enno; Slawin, Alexandra M. Z.; Mebs, Stefan; Woollins, J. Derek; Beckmann, Jens
Journal of publication
Organometallics
Year of publication
2017
a
9.4121 ± 0.0006 Å
b
12.0423 ± 0.0008 Å
c
32.192 ± 0.002 Å
α
90°
β
97.159 ± 0.002°
γ
90°
Cell volume
3620.3 ± 0.4 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1302
Residual factor for significantly intense reflections
0.0749
Weighted residual factors for significantly intense reflections
0.1784
Weighted residual factors for all reflections included in the refinement
0.1927
Goodness-of-fit parameter for all reflections included in the refinement
