Information card for entry 4089211

Structure parameters

• Formula: C18 H48 N3 Si3 Y
• Calculated formula: C18 H48 N3 Si3 Y
• SMILES: [Y]123([H][Si](C)(C)N1C(C)(C)C)([H][Si](C)(C)N2C(C)(C)C)[H][Si](C)(C)N3C(C)(C)C
• Title of publication: β-SiH-Containing Tris(silazido) Rare-Earth Complexes as Homogeneous and Grafted Single-Site Catalyst Precursors for Hydroamination
• Authors of publication: Eedugurala, Naresh; Wang, Zhuoran; Yan, KaKing; Boteju, Kasuni C.; Chaudhary, Umesh; Kobayashi, Takeshi; Ellern, Arkady; Slowing, Igor I.; Pruski, Marek; Sadow, Aaron D.
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 6
• Pages of publication: 1142
• a: 11.1827 ± 0.0005 Å
• b: 14.4439 ± 0.0007 Å
• c: 17.9963 ± 0.0008 Å
• α: 90°
• β: 90.992 ± 0.002°
• γ: 90°
• Cell volume: 2906.4 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0873
• Weighted residual factors for all reflections included in the refinement: 0.0875
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No