Information card for entry 4089212

Structure parameters

• Formula: C22 H58 N3 O Si3 Y
• Calculated formula: C22 H58 N3 O Si3 Y
• SMILES: [Y]123(N(C(C)(C)C)[Si](C)(C)[H]1)(N(C(C)(C)C)[Si](C)(C)[H]2)(N(C(C)(C)C)[Si](C)(C)[H]3)[O](CC)CC
• Title of publication: β-SiH-Containing Tris(silazido) Rare-Earth Complexes as Homogeneous and Grafted Single-Site Catalyst Precursors for Hydroamination
• Authors of publication: Eedugurala, Naresh; Wang, Zhuoran; Yan, KaKing; Boteju, Kasuni C.; Chaudhary, Umesh; Kobayashi, Takeshi; Ellern, Arkady; Slowing, Igor I.; Pruski, Marek; Sadow, Aaron D.
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 6
• Pages of publication: 1142
• a: 19.229 ± 0.002 Å
• b: 10.9623 ± 0.0012 Å
• c: 16.9486 ± 0.0018 Å
• α: 90°
• β: 114.423 ± 0.002°
• γ: 90°
• Cell volume: 3253 ± 0.6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1174
• Weighted residual factors for all reflections included in the refinement: 0.1214
• Goodness-of-fit parameter for all reflections included in the refinement: 1.197
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No