Information card for entry 4089524

Structure parameters

• Formula: C16 H16 As O10 P W2
• Calculated formula: C16 H16 As O10 P W2
• SMILES: [W]([AsH]([W](C#[O])(C#[O])(C#[O])(C#[O])C#[O])[PH](C(C)C)C(C)C)(C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Versatile Reactivity of Bridged Pentelidene Complexes toward Secondary and Tertiary Phosphines
• Authors of publication: Stubenhofer, Markus; Kuntz, Christian; Bodensteiner, Michael; Timoshkin, Alexey Y.; Scheer, Manfred
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 12
• Pages of publication: 3521
• a: 10.4709 ± 0.0001 Å
• b: 13.8828 ± 0.0002 Å
• c: 16.3691 ± 0.0002 Å
• α: 90°
• β: 92.908 ± 0.001°
• γ: 90°
• Cell volume: 2376.44 ± 0.05 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0529
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1278
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No