Information card for entry 4104481

Structure parameters

• Formula: C11 H30 Br N P2 Si
• Calculated formula: C11 H29.75 Br N P2 Si
• SMILES: [Br-].[Si](N=P([P+](CC)(CC)CC)(C)C)(C)(C)C
• Title of publication: Synthesis and Reactivity of Phosphine-Stabilized Phosphoranimine Cations, [R3P.PR'2=NSiMe3]+
• Authors of publication: Keith Huynh; Alan J. Lough; Michelle A. M. Forgeron; Martin Bendle; Alejandro Presa Soto; Roderick E. Wasylishen; Ian Manners
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 7905 - 7916
• a: 14.0798 ± 0.0007 Å
• b: 17.0889 ± 0.0008 Å
• c: 18.0705 ± 0.0006 Å
• α: 118.17 ± 0.002°
• β: 104.297 ± 0.003°
• γ: 90.164 ± 0.002°
• Cell volume: 3677.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1966
• Residual factor for significantly intense reflections: 0.1478
• Weighted residual factors for significantly intense reflections: 0.4397
• Weighted residual factors for all reflections included in the refinement: 0.4493
• Goodness-of-fit parameter for all reflections included in the refinement: 2.564
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No