Information card for entry 4105536

Structure parameters

• Chemical name: catena-(di(hexafluoroacetylacetonate)-zinc(II)- di(hexafluoroacetylacetonate)-lead(II))
• Formula: C20 H4 F24 O8 Pb Zn
• Calculated formula: C20 H4 F24 O8 Pb Zn
• Title of publication: Fluorinated Heterometallic β-Diketonates as Volatile Single-Source Precursors for the Synthesis of Low-Valent Mixed-Metal Fluorides
• Authors of publication: Anantharamulu Navulla; Alexander A. Tsirlin; Artem M. Abakumov; Roman V. Shpanchenko; Haitao Zhang; Evgeny V. Dikarev
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 692 - 694
• a: 18.398 ± 0.0016 Å
• b: 14.4711 ± 0.0013 Å
• c: 23.748 ± 0.002 Å
• α: 90°
• β: 107.307 ± 0.001°
• γ: 90°
• Cell volume: 6036.4 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1222
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No