Information card for entry 4105537

Structure parameters

• Chemical name: catena-(di(hexafluoroacetylacetonate)-nickel(II)- di(hexafluoroacetylacetonate)-lead(II))
• Formula: C20 H4 F24 Ni O8 Pb
• Calculated formula: C20 H4 F24 Ni O8 Pb
• Title of publication: Fluorinated Heterometallic β-Diketonates as Volatile Single-Source Precursors for the Synthesis of Low-Valent Mixed-Metal Fluorides
• Authors of publication: Anantharamulu Navulla; Alexander A. Tsirlin; Artem M. Abakumov; Roman V. Shpanchenko; Haitao Zhang; Evgeny V. Dikarev
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 692 - 694
• a: 18.4611 ± 0.0016 Å
• b: 12.6354 ± 0.0011 Å
• c: 13.6823 ± 0.0011 Å
• α: 90°
• β: 97.755 ± 0.001°
• γ: 90°
• Cell volume: 3162.4 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0625
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1433
• Weighted residual factors for all reflections included in the refinement: 0.1516
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No