Fluorine for Hydrogen Exchange in the Hydrofluorobenzene Derivatives C6HxF(6-x), where x= 2, 3, 4 and 5 by Monomeric [1,2,4-(Me3C)3C5H2]2CeH: The Solid State Isomerization of [1,2,4-(Me3C)3C5H2]2Ce(2,3,4,5-C6HF4) to [1,2,4-(Me3C)3C5H2]2Ce(2,3,4,6-C6HF4)
Authors of publication
Evan L. Werkema; Richard A. Andersen
Journal of publication
Journal of the American Chemical Society
Year of publication
2008
Journal volume
130
Pages of publication
7153 - 7165
a
10.1818 ± 0.0005 Å
b
22.164 ± 0.001 Å
c
17.8504 ± 0.0009 Å
α
90°
β
91.591 ± 0.001°
γ
90°
Cell volume
4026.7 ± 0.3 Å3
Cell temperature
169.2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0453
Residual factor for significantly intense reflections
0.0382
Weighted residual factors for all reflections
0.0557
Weighted residual factors for all reflections included in the refinement
0.0546
Goodness-of-fit parameter for all reflections included in the refinement
