Fluorine for Hydrogen Exchange in the Hydrofluorobenzene Derivatives C6HxF(6-x), where x= 2, 3, 4 and 5 by Monomeric [1,2,4-(Me3C)3C5H2]2CeH: The Solid State Isomerization of [1,2,4-(Me3C)3C5H2]2Ce(2,3,4,5-C6HF4) to [1,2,4-(Me3C)3C5H2]2Ce(2,3,4,6-C6HF4)
Authors of publication
Evan L. Werkema; Richard A. Andersen
Journal of publication
Journal of the American Chemical Society
Year of publication
2008
Journal volume
130
Pages of publication
7153 - 7165
a
10.221 ± 0.0006 Å
b
22.063 ± 0.001 Å
c
18.024 ± 0.001 Å
α
90°
β
92.369 ± 0.001°
γ
90°
Cell volume
4061 ± 0.4 Å3
Cell temperature
158.2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0404
Residual factor for significantly intense reflections
0.0305
Weighted residual factors for all reflections
0.0415
Weighted residual factors for all reflections included in the refinement
0.0401
Goodness-of-fit parameter for all reflections included in the refinement
