Crystallography Open Database

Information card for entry 4113975

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Coordinates	4113975.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H43 P3 Ru Si2
Calculated formula	C21 P3 Ru Si2
Title of publication	Structure and Reactivity of Bis(silyl) Dihydride Complexes (PMe3)3Ru(SiR3)2(H)2: Model Compounds and Real Intermediates in a Dehydrogenative C-Si Bond Forming Reaction
Authors of publication	Vladimir K. Dioumaev; Bok R. Yoo; Leo J. Procopio; Patrick J. Carroll; Donald H. Berry
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	8936 - 8948
a	18.029 ± 0.0006 Å
b	16.2315 ± 0.0006 Å
c	9.5547 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2796.07 ± 0.18 Å³
Cell temperature	273.2 K
Ambient diffraction temperature	273.2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for significantly intense reflections	0.042
Weighted residual factors for significantly intense reflections	0.05
Goodness-of-fit parameter for significantly intense reflections	1.58
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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