Crystallography Open Database

Information card for entry 4119839

4119838 << 4119839 >> 4119840

Preview

Coordinates	4119839.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C103.67 H120.67 Cu2 F12 N8 O31 Rh4 S4
Calculated formula	C96.6667 H92 Cu2 F11 N8 O26 Rh4 S3.66667
Title of publication	Cp*Rh-Based Heterometallic Metallarectangles: Size-Dependent Borromean Link Structures and Catalytic Acyl Transfer
Authors of publication	Sheng-Li Huang; Yue-Jian Lin; T. S. Andy Hor; Guo-Xin Jin
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	8125 - 8128
a	41.014 ± 0.0008 Å
b	23.7783 ± 0.0004 Å
c	37.6234 ± 0.0007 Å
α	90°
β	103.62 ± 0.001°
γ	90°
Cell volume	35660.1 ± 1.1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1273
Residual factor for significantly intense reflections	0.0972
Weighted residual factors for significantly intense reflections	0.2704
Weighted residual factors for all reflections included in the refinement	0.301
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4119839.html