Information card for entry 4119840

Structure parameters

• Formula: C73 H90 Cu2 F6 N10 O25.33 Rh4 S2
• Calculated formula: C72 H86 Cu2 F3 N10 O22.3333 Rh4 S
• Title of publication: Cp*Rh-Based Heterometallic Metallarectangles: Size-Dependent Borromean Link Structures and Catalytic Acyl Transfer
• Authors of publication: Sheng-Li Huang; Yue-Jian Lin; T. S. Andy Hor; Guo-Xin Jin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 8125 - 8128
• a: 35.098 ± 0.003 Å
• b: 35.098 ± 0.003 Å
• c: 15.8896 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 16952 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 173
• Hermann-Mauguin space group symbol: P 63
• Hall space group symbol: P 6c
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.164
• Weighted residual factors for all reflections included in the refinement: 0.1788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No