Crystallography Open Database

Information card for entry 4119841

4119840 << 4119841 >> 4119842

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Coordinates	4119841.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C92 H118 Cu2 F12 N10 O34 Rh4 S4
Calculated formula	C88 H98 Cu2 N10 O22 Rh4
Title of publication	Cp*Rh-Based Heterometallic Metallarectangles: Size-Dependent Borromean Link Structures and Catalytic Acyl Transfer
Authors of publication	Sheng-Li Huang; Yue-Jian Lin; T. S. Andy Hor; Guo-Xin Jin
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	8125 - 8128
a	11.0061 ± 0.001 Å
b	16.7944 ± 0.0015 Å
c	30.67 ± 0.003 Å
α	90°
β	96.107 ± 0.002°
γ	90°
Cell volume	5636.9 ± 0.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1155
Residual factor for significantly intense reflections	0.0753
Weighted residual factors for significantly intense reflections	0.2089
Weighted residual factors for all reflections included in the refinement	0.2308
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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