Information card for entry 4120341

Structure parameters

• Formula: C49 H77 Ge N2
• Calculated formula: C49 H77 Ge N2
• Title of publication: Acyclic Germylones: Congeners of Allenes with a Central Germanium Atom
• Authors of publication: Yan Li; Kartik Chandra Mondal; Herbert W. Roesky; Hongping Zhu; Peter Stollberg; Regine Herbst-Irmer; Dietmar Stalke; Diego M. Andrada
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 12422 - 12428
• a: 9.29 ± 0.002 Å
• b: 12.091 ± 0.002 Å
• c: 19.902 ± 0.003 Å
• α: 94.809 ± 0.004°
• β: 98.576 ± 0.004°
• γ: 97.669 ± 0.004°
• Cell volume: 2178.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0936
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes