Information card for entry 4120342

Structure parameters

• Formula: C43 H69 Ge N2
• Calculated formula: C43 H69 Ge N2
• Title of publication: Acyclic Germylones: Congeners of Allenes with a Central Germanium Atom
• Authors of publication: Yan Li; Kartik Chandra Mondal; Herbert W. Roesky; Hongping Zhu; Peter Stollberg; Regine Herbst-Irmer; Dietmar Stalke; Diego M. Andrada
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 12422 - 12428
• a: 9.161 ± 0.002 Å
• b: 19.325 ± 0.003 Å
• c: 24.76 ± 0.003 Å
• α: 112.3 ± 0.03°
• β: 98.13 ± 0.02°
• γ: 91.48 ± 0.02°
• Cell volume: 3999.7 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0713
• Weighted residual factors for all reflections included in the refinement: 0.0755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes