Information card for entry 4124277

Structure parameters

• Formula: C42 H95 K N4 O6 Si6 Th
• Calculated formula: C42 H95 K N4 O6 Si6 Th
• Title of publication: Thorium Mono- and Bis(imido) Complexes Made by Reprotonation of cyclo-Metalated Amides.
• Authors of publication: Bell, Nicola L.; Maron, Laurent; Arnold, Polly L.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Pages of publication: 150814165612001
• a: 12.2166 ± 0.0004 Å
• b: 14.0289 ± 0.0005 Å
• c: 19.5008 ± 0.0007 Å
• α: 84.295 ± 0.003°
• β: 82.139 ± 0.003°
• γ: 71.601 ± 0.003°
• Cell volume: 3135.9 ± 0.2 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0744
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.0757
• Weighted residual factors for all reflections included in the refinement: 0.0828
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No