Information card for entry 4124278

Structure parameters

• Formula: C44 H86 K2 N4 O2 Si4 Th
• Calculated formula: C44 H86 K2 N4 O2 Si4 Th
• Title of publication: Thorium Mono- and Bis(imido) Complexes Made by Reprotonation of cyclo-Metalated Amides.
• Authors of publication: Bell, Nicola L.; Maron, Laurent; Arnold, Polly L.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Pages of publication: 150814165612001
• a: 13.1981 ± 0.0003 Å
• b: 13.8897 ± 0.0003 Å
• c: 18.8942 ± 0.0004 Å
• α: 94.64 ± 0.002°
• β: 94.357 ± 0.002°
• γ: 116.604 ± 0.002°
• Cell volume: 3062.21 ± 0.13 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.089
• Weighted residual factors for all reflections included in the refinement: 0.0927
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No