Information card for entry 4127068

Structure parameters

• Formula: C89 H92 B2 Cl10 O2 P4 Rh2
• Calculated formula: C89 H92 B2 Cl10 O2 P4 Rh2
• Title of publication: Dehydropolymerization of H3B·NMeH2 To Form Polyaminoboranes Using [Rh(Xantphos-alkyl)] Catalysts.
• Authors of publication: Adams, Gemma M.; Colebatch, Annie L.; Skornia, Joseph T.; McKay, Alasdair I.; Johnson, Heather C.; Lloyd Jones, Guy C.; Macgregor, Stuart A.; Beattie, Nicholas A.; Weller, Andrew S.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• a: 14.1034 ± 0.0004 Å
• b: 14.4749 ± 0.0009 Å
• c: 23.9437 ± 0.001 Å
• α: 82.527 ± 0.004°
• β: 85.664 ± 0.003°
• γ: 83.694 ± 0.003°
• Cell volume: 4807.8 ± 0.4 ų
• Cell temperature: 150 ± 0.4 K
• Ambient diffraction temperature: 150 ± 0.4 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1125
• Residual factor for significantly intense reflections: 0.0787
• Weighted residual factors for significantly intense reflections: 0.1904
• Weighted residual factors for all reflections included in the refinement: 0.2255
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No