Information card for entry 4127549

Structure parameters

• Formula: C51 H101 B Co I Na O6 P3
• Calculated formula: C51 H101 B Co I Na O6 P3
• Title of publication: Activations of all Bonds to Silicon (Si-H, Si-C) in a Silane with Extrusion of [CoSiCo] Silicide Cores.
• Authors of publication: Handford, Rex C.; Smith, Patrick W.; Tilley, T. Don
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 22
• Pages of publication: 8769 - 8772
• a: 11.4364 ± 0.0013 Å
• b: 15.6713 ± 0.0018 Å
• c: 16.661 ± 0.002 Å
• α: 90.509 ± 0.006°
• β: 91.262 ± 0.007°
• γ: 98.341 ± 0.006°
• Cell volume: 2953.5 ± 0.6 ų
• Cell temperature: 104 K
• Ambient diffraction temperature: 104.57 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0784
• Residual factor for significantly intense reflections: 0.0633
• Weighted residual factors for significantly intense reflections: 0.1419
• Weighted residual factors for all reflections included in the refinement: 0.1489
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No