Crystallography Open Database

Information card for entry 4131465

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Coordinates	4131465.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H18 I2 N8 Pd2
Calculated formula	C22 H18 I2 N8 Pd2
Title of publication	Tuning the Stability of Pd(IV) Intermediates Using a Redox Non-innocent Ligand Combined with an Organolanthanide Fragment.
Authors of publication	Goudy, Violaine; Jaoul, Arnaud; Cordier, Marie; Clavaguéra, Carine; Nocton, Grégory
Journal of publication	Journal of the American Chemical Society
Year of publication	2017
Journal volume	139
Journal issue	31
Pages of publication	10633 - 10636
a	10.4545 ± 0.0005 Å
b	17.5951 ± 0.0007 Å
c	13.9967 ± 0.0008 Å
α	90°
β	110.081 ± 0.002°
γ	90°
Cell volume	2418.1 ± 0.2 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1032
Residual factor for significantly intense reflections	0.0823
Weighted residual factors for significantly intense reflections	0.1975
Weighted residual factors for all reflections included in the refinement	0.215
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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