Crystallography Open Database

Information card for entry 4131466

Preview

Coordinates	4131466.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H69 I N4 Pd Yb
Calculated formula	C31 H45 I N4 Pd Yb
Title of publication	Tuning the Stability of Pd(IV) Intermediates Using a Redox Non-innocent Ligand Combined with an Organolanthanide Fragment.
Authors of publication	Goudy, Violaine; Jaoul, Arnaud; Cordier, Marie; Clavaguéra, Carine; Nocton, Grégory
Journal of publication	Journal of the American Chemical Society
Year of publication	2017
Journal volume	139
Journal issue	31
Pages of publication	10633 - 10636
a	27.1623 ± 0.0009 Å
b	12.2012 ± 0.0005 Å
c	15.2011 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	5037.8 ± 0.3 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0548
Residual factor for significantly intense reflections	0.0412
Weighted residual factors for significantly intense reflections	0.116
Weighted residual factors for all reflections included in the refinement	0.1224
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4131466.html