Information card for entry 4300801

Structure parameters

• Common name: [(Dipp*GeNH2)2].1.5toluene
• Formula: C70.5 H90 Ge2 N2
• Calculated formula: C70.5 H90 Ge2 N2
• Title of publication: Synthesis and Characterization of Ge(II), Sn(II), and Pb(II) Monoamides with -NH2 Ligands
• Authors of publication: Stanciu, Corneliu; Hino, Shirley S.; Stender, Matthias; Richards, Anne F.; Olmstead, Marilyn M.; Power, Philip P.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Journal issue: 8
• Pages of publication: 2774 - 2780
• a: 43.49 ± 0.005 Å
• b: 16.84 ± 0.002 Å
• c: 18.469 ± 0.002 Å
• α: 90°
• β: 114.265 ± 0.002°
• γ: 90°
• Cell volume: 12331 ± 2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0784
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1017
• Weighted residual factors for all reflections included in the refinement: 0.127
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No