Information card for entry 4301668

Structure parameters

• Formula: C84 H130 Ge2 N2 Sn2
• Calculated formula: C84 H130 Ge2 N2 Sn2
• Title of publication: N-H and N=C Bond Formation via Germanium(III) Diradicaloid Intermediates and C-S Bond Cleavage in Reactions of the Digermyne Ar'GeGeAr' (Ar' = C6H3-2,6-(C6H3-2,6-Pri2)2) with Azides
• Authors of publication: Xinping Wang; Chengbao Ni; Zhongliang Zhu; James C. Fettinger; Philip P. Power
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2464 - 2470
• a: 23.0657 ± 0.0011 Å
• b: 21.0954 ± 0.001 Å
• c: 32.2509 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15692.6 ± 1.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0669
• Weighted residual factors for all reflections included in the refinement: 0.0736
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No