Information card for entry 4302488

Structure parameters

• Formula: H58.3 Mo3 Ni1.85 O90 P2 W15
• Calculated formula: Mo3.019 Ni1.837 O90 P2 W14.981
• Title of publication: 2D and 3D Polymeric Wells-Dawson Polyoxometelates: Synthesis, Crystal Structures, and Cyclic Voltammetry of [(M(H2O)4)x][H6-2xP2W18-nMonO62] (M = CuII, CoII, NiII)
• Authors of publication: Robila Belghiche; Ouahiba Bechiri; Mostefa Abbessi; Stéphane Golhen; Yann Le Gal; Lahcène Ouahab
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6026 - 6033
• a: 12.916 ± 0.001 Å
• b: 14.663 ± 0.001 Å
• c: 20.977 ± 0.001 Å
• α: 84.956 ± 0.01°
• β: 88.707 ± 0.01°
• γ: 66.299 ± 0.01°
• Cell volume: 3623.3 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.1124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No