Information card for entry 4302489

Structure parameters

• Formula: Cu2.5 H43.67 O83.33 P2 W18
• Calculated formula: Cu2.502 O83.168 P2 W18
• Title of publication: 2D and 3D Polymeric Wells-Dawson Polyoxometelates: Synthesis, Crystal Structures, and Cyclic Voltammetry of [(M(H2O)4)x][H6-2xP2W18-nMonO62] (M = CuII, CoII, NiII)
• Authors of publication: Robila Belghiche; Ouahiba Bechiri; Mostefa Abbessi; Stéphane Golhen; Yann Le Gal; Lahcène Ouahab
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6026 - 6033
• a: 15.289 ± 0.0009 Å
• b: 15.289 ± 0.0009 Å
• c: 55.98 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 11332.4 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0597
• Weighted residual factors for all reflections included in the refinement: 0.0699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No